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The Research Journal of the Costume Culture = 복식문화연구 v.20 no.2, 2012년, pp.238 - 250   피인용횟수: 1
본 등재정보는 저널의 등재정보를 참고하여 보여주는 베타서비스로 정확한 논문의 등재여부는 등재기관에 확인하시기 바랍니다.

과산화수소/자외선/산소 처리를 이용한 베르베린 염료 및 염직물의 퇴화거동 연구
Study on the Degradation Behavior of Berberine Dye and Berberine Dyed Silk using Hydrogen Peroxide/UV/Oxygen Treatment

안춘순    (인천대학교 패션산업학과  );
  • 초록

    This study examined the degradation behavior of SB(standard berberine) dye and SB dyed silk using HPLC-MS instrument after degradation in the hydrogen peroxide/ultraviolet ray radiation/oxygen system up to 9 days and 40 hours respectively. In the degraded samples, berberine was detected at 5.2 min in the SB dye and 5.3 min in the SB dyed silk with its molecular ion=336 and the UV spectra of quaternary alkaloid. Degradation product 3(m/z=102) newly appeared after 5 day degradation treatment with continued increase till the end of degradation treatment. The amount of berberine in the degraded dye decreased with degradation progression. In the silk dyeings, berberine was detected only up to 21 hour degradation sample. The amount of berberine decreased dramatically during the first 6 hours of degradation treatment. The CIELAB color measurement of the silk dyeings showed dramatic change in the b* value, near zero in the 40 hour degraded silk. CIELAB and Munsell color measurements were in agreement with the HPLC-MS results of the dyed silk in the change of berberine content that the degraded silk became white and lost yellow color.


  • 주제어

    베르베린 .   퇴화 .   황백 .   고속 액체 크로마토 그라피 질량분석 .   측색.  

  • 참고문헌 (43)

    1. Ahn, C.(2006). 영암군 금정면 탐진최씨 출토복식 분석[Analysis of exhumed textiles of Tamjin Choi of Kumjungmyeon, Youngamgoon]. In Ewha Womans University Museum (Ed.), 최원립 장군묘 출토복식을 통해 본 17세기 조선 무관의 차림새[The 17th-century Joseon military attire excavated from the tomb of General Choi Won-Lip] (pp. 206-222). Seoul: Minsokwon. 
    2. Ahn, C.(2009). Examination of berberine dye using GC-MS after selective degradation treatments. Journal of the Korean Society of Clothing and Textiles, 33(12), 2002-2010.     
    3. Ahn, C.(2010). GC-MS analysis of amur cork tree extract and its degradation products. Journal of the Koreean Society of Clothing and Textiles, 34(6), 1042-1052.     
    4. Ahn, C.(2011). Analysis of dye extracted from Phellodendron bark using liquid chromatography. Journal of the Korean Society of Clothing and Textiles, 35(12), in print.     
    5. Ahn, C., & Obendorf, S. K.(2004). Dyes on archaeological textiles: Analyzing alizarin and its degradation products. Textiles Research Journal, 74(11), 949-954. 
    6. Ahn, C., & Obendorf, S. K.(2007). GC-MS analysis of curcumin dye after selective degradation treatment. Fibers and Polymers, 8(3), 278-283.     
    7. Ahn, C., Zeng, X., & Obendorf, S. K.(in print). Analysis of dye extracted from Phellodendron bark and its identification in archaeological textiles. Textile Research Journal. 
    8. Berghe, I. V., Gleba, M., & Mannering, U.(2009). Towards the identification of dyestuffs in early Iron Age Scandinavian peat bog textiles. Journal of Archaeological Science, 36(9), 1910-1921. 
    9. Chan, C. O., Chu, C. C., Mok, D. K. W., & Chau, F. T.(2007). Analysis of berberine and total alkaloid content in Cortex Phellodendri by near infrared spectroscopy (NIRS) compared with high-performance liquid chromatography coupled with ultravisible spectrometric detection. Analytica Chimica Acta, 592(2), 121-131. 
    10. Choo, C. K. K., & Lee, Y. E.(2002). Analysis of dyeings produced by traditional Korean methods using colorants from plant extracts. Coloration Technology, 118(1), 35-45. 
    11. Colonna, G. M., Caronna, T., Marcandalli, B.(1999). Oxidative degradation of dyes by ultraviolet radiation in the presence of hydrogen peroxide. Dyes and Pigments, 41(3), 211-220. 
    12. Cooper, W. J., & Lean, D. R. S.(1989). Hydrogen peroxide concentration in a northern lake: Photochemical formation and dial variability. Environmental Science & Technology, 23(11), 1425-1428. 
    13. Drasar, P., & Moravcova, J.(2004). Recent advances in analysis of Chinese medical plantsand traditional medicines. Journal of Chromatography B, 812(1/2), 3-21. 
    14. Petroviciu, I., Albu, F., & Medvedovici, A.(2010). LC/MS and LC/MS/MS based protocol for identification of dyes in historic textiles. Microchemical Journal, 95(2), 247-254. 
    15. Grosjean, D., Whitmore, P. M., Moor, P. D., Cass, G. R., & Druzik, J. R.(1988). Ozone fading of organic colorants: Products and mechanism of the reaction of ozone with curcumin. Environmental Science and Technology, 22(11), 1357-1361. 
    16. Hu, Y. M., Su, G. H., Sze, S. C. W., Ye, W., & Tong, Y.(2010). Quality assessment of Cortex Phellodendri by high-performance liquid chromatography coupled with electrospray ionization mass spectrometry. Biomedical Chromatography, 24(4), 438-453. 
    17. Hua, W., Ding, L., Chen, Y., Gong, C. B., He, J., & Xu, G.(2007). Determination of berberine in human plasma by liquid chromatography-electrospray ionization-mass spectrometry. Journal of Pharmaceutical and Biomedical Analysis, 44(4), 931-937. 
    18. Ince, N. H.(1999). Critical effect of hydrogen peroxide in photochemical dye degradation. Water Research, 33(4), 1080-1084. 
    19. Jarosz-Wilkolazka, A., Kochmanska-Rdest, J., Malarczyk, E., Wardas, W., & Leonowicz, A.(2002). Fungi and their ability to decolourize azo and anthraquinonic dyes. Enzyme and Microbial Technology, 30(4), 566-572. 
    20. Jung, W. K., Chang, D. S., Seol, B. Y., Park, S. J., Cho, I. S., & Cho, K. M.(1997). 염색학[Studies on dyeing]. Seoul: Hyungseul Publishing Co. 
    21. Kim, S. J., Ishikawa, K., Hirai, M., & Shoda, M. (1995). Characteristics of a newly isolated fungus, Geotrichum candidum Dec1, which decolorizes various dyes. Journal of Fermentation and Bioengineering, 79(6), 601-607. 
    22. Kim, T. K., Yoon, S. H., Lim, Y. J., & Son, Y. A. (2003). Dyeability improvement of berberine colorant by electrostatic attactive force of a reactive anionic agent. Journal of the Korean Society of Dyers and Finishers, 158(6), 47-54. 
    23. Lee, H. S., Eom, Y. E., & Eom, D. O.(1999). Narrowbore high performance liquid chromatography of berberine and palmatine in crude drugs and pharmaceuticals with ion-pair extraction using cobalt thiocyanate reagent. Journal of Pharmaceutical and Biomedical Analysis, 21(1), 59-63. 
    24. Lee, J. G., Choi, J. Y., Oh, J. S., Jung, H. W., Choi, E. H., Lee, H. S., Kim, J. A., Chang, T. S., Son, J. K., & Lee, S. H.(2007). Isolation of melamin biosynthesis inhibitory compounds from the Phellodendri Cortex. Korean Journal of Pharmacognosy, 38(4), 387-393. 
    25. Lee, M. S., Hong, M. K., Kim, E. K., & Bae, S. W. (2001). Effect of storage conditions on the color and the mechanical properties of fabrics dyed with natural dyes. Journal of the Korean Society of Clothing and Textiles, 25(3), 617-628. 
    26. Lee, Y. H., Hwang, E. K., Jung, Y. J., Do, S. K., & Kim, H. D.(2010). Dyeing and deodorizing properties of cotton, silk, wool fabrics dyed with Amur Corktree, Dryopteris crassirhizoma, Chrysanthemum boreale, Artemisia extracts. Journal of Applied Polymer Science, 115(4), 2246-2253. 
    27. Lee, Y., Lee, J., Kim, Y., Choi, S., Ham, S. W., & Kim, K. J.(2008). Investigation of natural dyes and ancient textiles from Korea using TOF-SIMS. Applied Surface Science, 255, 1033-1036. 
    28. Li, X., Liu, H., Li, J., Zhao, X., Wang, S., & Zheng, X.(2009). Simultaneous determination of berberine and palmatine in rabbit plasma by LC-MS-MS and its application in pharmacokinetic study after oral administration of coptidis and coptidisgardeniae couple extract. Chromatographia, 70(7/8), 1113-1119. 
    29. Li, X., Wang, Y., & Yan, X.(2007). Effects of water stress on berberine, jatrorrhizine and palmatine contents in amur corktree seedlings. Acta Ecologica Sinica, 27(1), 58-64. 
    30. Liu, G., Wu, T., & Zhao, J.(1999). Photoassisted degradation of dye pollutants. Irreversible degradation of alizarin red under visible light radiation in air-equilibrated aqueous $TiO_{2}$ dispersions. Environmental Science and Technology, 33(12), 2081-2087. 
    31. Nyanhongo, G. S., Gomes, J., Gubitz, G. M., Zvauya, R., Read, J., & Steiner, W.(2002). Decolorization of textile dyes by laccases from a newly isolated strain of Trametes modesta. Water Research, 36(2), 1449-1456. 
    32. Needles, H. L., & Nowak, K. C. J.(1989). Heatinduced aging of linen. In S. H. Zeronian & H. L. Needles (Eds), Historic textile and paper materials II: Conservation and characterization, ACS Symposium series 410 (pp. 159-167). Washington, DC: American Chemical Society. 
    33. Park, S. S.(1998). 파주 금릉리 출토 경주정씨 유물 소고[Study on the textiles of Kyungju Chung family excavated from Kumreungri Pajoo]. 한국복식[Korean Costume], 16, 31-89. 
    34. Peacock, E. E.(1996). Biodegradation and characterization of water-degraded archaeological textiles created for conservation research. International Biodeterioration and Biodegradation, 38(1), 49-59. 
    35. Peralta-Zamora, P., Kunz Moraes, S. G. de., Perlegrini, R., Moleiro, P. C., Reyes, J., & Duran, N.(1999). Degradation of reactive dyes. I. Comparative study of ozonation, enzymatic and photochemical processes. Chemosphere, 38(4), 835-852. 
    36. Read, R. A., & Zasada, J. C.(2008). Phellodendron amurense Rupr.: Amur corktree. In Bonner Franklin T., Karrfalt, Robert P. (Eds.), The woody plant seed manual, agric. handbook No. 727 (pp. 783-785). Washington, DC: US Department of Agriculture, Forest Service. 
    37. Scheck, C. K., & Frimmel, F. H.(1995). Degradation of phenol and salicylic acid by ultraviolet radiation/ hydrogen peroxide/oxygen. Water Research, 29(10), 2346-2352. 
    38. Schweppe, H.(1989). Identification of red madder and insect dyes by thin-layer chromatography. In ACS Symposium Series 410, S. H. Zeronian and H. L. Needles, Eds., American Chemical Society, Washington, D.C., pp. 188-219. 
    39. Suto, K., Kakinuma, S., Ito, Y., Sagara, K., Iwasaki, H., & Itokawa, H.(1997). Determination of berberine and palmatine in Phellodendri Cortex using ion-pair supercritical fluid chromatography on-line coupled with ion-pair supercritical fluid extraction by on-column trapping. Journal of Chromatography A, 786(2), 371-376. 
    40. Wang, Y. J., Pan, M. H., Cheng, A. L., Lin, L. I., Ho, Y. S., Hsieh, C. Y., & Lin, J. K.(1997). Stability of curcumin in buffer solutions and characterization of its degradation products. Journal of Pharmaceutical and Biomedical Analysis, 15(12), 1867-1876. 
    41. Wouters, J.(1985). High performance liquid chromatography of anthraquinones: Analysis of plant and insect extracts and dyed textiles. Studies in Conservation, 30(3), 119-128. 
    42. Young, L., & Yu, J.(1997). Ligninase-catalysed decolorization of synthetic dyes. Water Research, 31(5), 1187-1193. 
    43. Zhang, X., Boytner, R., Cabrera, J. L., & Laursen, R. (2007). Identification of yellow dye types in Pre- Columbian Andean textiles. Analytical Chemistry, 79, 1575-1582. 
  • 이 논문을 인용한 문헌 (1)

    1. Li, Longchun ; Ahn, Cheunsoon 2014. "Comparison of Hwangbek Dyeability for Cotton, Silk, and Wool from Different Tree Species and Origin" 한국의류학회지 = Journal of the Korean Society of Clothing and Textiles, 38(1): 110~122     

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