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Organic letters v.19 no.2, 2017년, pp.376 - 379   SCI SCIE
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Trichloroisocyanuric Acid Promoted Cascade Cyclization/Trifluoromethylation of Allylic Oximes: Synthesis of Trifluoromethylated Isoxazolines

Zhang, Weigang (College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Su, Yingpeng ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Wang, Ke-Hu ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Wu, Lili ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Chang, Bingbing ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Shi, Ya ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Huang, Danfeng ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, ); Hu, Yulai ( College of Chemistry and Chemical Engineering, Northwest Normal University, 967 Anning East Road, Lanzhou 730070, );
  • 초록  

    Cheap and commercially available trichloroisocyanuric acid has been used to promote trifluoromethylation by using TMSCF 3 as the trifluoromethyl source. The method provides a novel and efficient protocol for the construction of CF 3 -containing 4,5-dihydroisoxazoles from allylic oximes in good to excellent yields. Graphic Abstract ACS Electronic Supporting Info


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