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Tetrahedron v.74 no.16, 2018년, pp.1991 - 2001   SCI SCIE SCOPUS
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Synthesis of N,N′-bridged azacalixarenes

Takemura, Hiroyuki (Department of Chemical and Biological Sciences, Faculty of Science, Japan Women's University, Mejirodai 2-8-1, Bunkyo-ku, Tokyo 112-8681, Japan ) ; Sako, Katsuya (Department of Life Science and Applied Chemistry, Nagoya Institute of Technology, Gokiso, Showa-ku, Nagoya 466-8555, Japan ) ; Iwanaga, Tesuo (Department of Chemistry, Faculty of Science, Okayama University of Science, 1-1 Ridaicho, Okayama 700-0005, Japan ) ; Tatsumi, Akane (Department of Chemical and Biological Sciences, Faculty of Science, Japan Women's University, Mejirodai 2-8-1, Bunkyo-ku, Tokyo 112-8681, Japan ) ; Mogami, Yukako (Department of Chemical and Biological Sciences, Faculty of Science, Japan Women's University, Mejirodai 2-8-1, Bunkyo-ku, Tokyo 112-8681, Japan ) ; Watanabe, Hiromi (Department of Chemical and Biological Sciences, Faculty of Science, Japan Women's University, Mejirodai 2-8-1, Bunkyo-ku, Tokyo 112-8681, Japan ) ; Aoki, Miho (Department of Chemical and Biological Sciences, Faculty of Science, Japan Women's University, Mejirodai 2-8-1, Bunkyo-ku, Tokyo 112-8681, Japan ) ; Yûki, Shiho (Department of Chemical and Bi ) ; Hayano, Yuri ; Itaka, Mirei ;
  • 초록  

    Abstract The one-pot reaction between bis(hydroxymethyl)phenol derivatives and diamines or triamines afforded novel azacalixarenes with bridged structures. Basket-type macrocycles of cone conformations, molecules that contained two aza[3.1.1.1]calixarene skeletons connected by a chain, or novel saucer-type azacalixarenes were obtained from the reaction. Structures of some of them were determined by crystallographic analyses. Highlights Bridged azacalixarenes. Calixarenes. Cyclophanes. Macrocycles. Supramolecular structures. Graphical abstract The Mannich-type one-pot condensation reaction between bis(hydroxymethyl)phenol derivatives and diamines afforded novel azacalixarenes with bridged structures in moderate yields without using hazardous benzyl halides. These novel structures are applicable to supramolecules and intercalates. Key Topic: Bridged azacalixarenes, one-pot synthesis, supramolecular structures. [DISPLAY OMISSION]


  • 주제어

    Azacyclophanes .   Azacalixarenes .   Calixarenes .   Macrocycles .   Cyclophanes.  

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