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Journal of the mechanical behavior of biomedical materials v.81, 2018년, pp.16 - 25   SCIE
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Strength and fracture mechanism of iron reinforced tricalcium phosphate cermet fabricated by spark plasma sintering

Tkachenko, Serhii (CEITEC - Central European Institute of Technology, Brno University of Technology, Brno, Czech Republic ) ; Horynová, Miroslava (CEITEC - Central European Institute of Technology, Brno University of Technology, Brno, Czech Republic ) ; Casas-Luna, Mariano (CEITEC - Central European Institute of Technology, Brno University of Technology, Brno, Czech Republic ) ; Diaz-de-la-Torre, Sebastian (CIITEC - Centro de Investigación e Innovación Tecnológica, Instituto Politécnico Nacional, Mexico City, Mexico ) ; Dvořák, Karel (Faculty of Civil Engineering, Brno University of Technology, Brno, Czech Republic ) ; Celko, Ladislav (CEITEC - Central European Institute of Technology, Brno University of Technology, Brno, Czech Republic ) ; Kaiser, Jozef (CEITEC - Central European Institute of Technology, Brno University of Technology, Brno, Czech Republic ) ; Montufar, Edgar B. (CEITEC - Central European Institute of Technology, Brno University of Technology, Brno, Czech Republic ) ;
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    Abstract The present work studies the microstructure and mechanical performance of tricalcium phosphate (TCP) based cermet toughened by iron particles. A novelty arises by the employment of spark plasma sintering for fabrication of the cermet. Results showed partial transformation of initial alpha TCP matrix to beta phase and the absence of oxidation of iron particles, as well as a lack of chemical reaction between TCP and iron components during sintering. The values of compressive and tensile strength of TCP/Fe cermet were 3.2 and 2.5 times, respectively, greater than those of monolithic TCP. Fracture analysis revealed the simultaneous action of crack-bridging and crack-deflection microstructural toughening mechanisms under compression. In contrast, under tension the reinforcing mechanism was only crack-bridging, being the reason for smaller increment of strength. Elastic properties of the cermet better matched values reported for human cortical bone. Thereby the new TCP/Fe cermet has potential for eventual use as a material for bone fractures fixation under load-bearing conditions. Highlights SPS improves the contact and anchorage of the Fe reinforcements with the TCP matrix. Addition of Fe increases 3.2 and 2.5 times the compressive and tensile strength of TCP. The main toughening mechanism in tension and compression is crack-bridging. In compression also crack-deflection toughening increases the strength of TCP. Fracture morphology of Fe in tension is dimpling while in compression is shear bands. Graphical abstract [DISPLAY OMISSION]


  • 주제어

    Ceramic-matrix composite .   Tricalcium phosphate .   Spark plasma sintering .   Microstructural toughening .   Fractography.  

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